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A straightforward green synthesis of N-(tert-butylsulfinyl)imines

Author:
Lv, Xirui  Zhou, Yue  Zhang, Anguo  Zhou, Lihong  Zeng, Qingle  


Journal:
TOXICOLOGICAL AND ENVIRONMENTAL CHEMISTRY


Issue Date:
2016


Abstract(summary):

A straightforward and environment-friendly protocol for the synthesis of valuable chiral N-(tert-butylsulfinyl)imines has been developed. Different from traditional process with benzaldehydes as substrates, arylmethyl alcohols, benzylthiol, dibenzyl ether, thioether, and disulfide are used as alternative substrates to react with tert-butanesulfinamide in the presence of (KOBu)-Bu-t under air for the synthesis of chiral N-(tert-butylsulfinyl)imines. This is a transition metal-free, mild, cost-effective, and simple process.


Page:
1155---1162


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