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Total synthesis of BE-43547A<sub>2</sub>

Author:
Yuanjun Sun  Xiuwen Su  Ruifei Zhou  Dehong Wang  Yuan Zhao  Yuhang Jiang  Liang Wang  Yue Chen  


Journal:
Tetrahedron


Issue Date:
2018


Abstract(summary):

Abstract An asymmetric total synthesis of BE-43547A 2 has been achieved in 16 steps (longest linear) on a 3.2 gram scale. The details of our efforts that led to the total synthesis of BE-43547A 2 were reported, the final 6 steps were optimized, and the overall yield was improved from 4.5% to 9.7%. The procedure utilized in the final 2 steps may serve as a better method for separating unstable APD compounds. Graphical abstract An asymmetric total synthesis of BE-43547A 2 has been achieved in 16 steps (longest linear) on a 3.2 gram scale. The details of our efforts that led to the total synthesis of BE-43547A 2 were reported, the final 6 steps were optimized, and the overall yield was improved from 4.5% to 9.7%. The procedure utilized in the final 2 steps may serve as a better method for separating unstable APD compounds. Image 1


Page:
5955-5955


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