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Purification of S-PG05 using Simulated Moving Bed Chromatography

Author:
Zhou, Weihong   Lan, Shaopeng   Wang, Jida   Lin, Bingchang  


Journal:
Separation Science and Technology


Issue Date:
2009


Abstract(summary):

S-PG05 ((15S)-15-methyl-prostaglandin F(2)alpha methyl ester) was separated from the epimer R-PG05 and other impurities using SMB, combined with batch chromatography. Based on this technical procedure, 94% pure S-PG05 was obtained. Different column configurations and separation conditions of SMB have been selected. A non-synchronous shift with a "partial extract withdrawal'' strategy has been employed, resulting in the saving of desorbent and the increase of the purity of S-PG05.


Page:
1510-1524


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